N,N,N-Trimethyl-1-ammonium adamantane

What is N,N,N-Trimethyl-1-ammonium adamantane, cas no:53075-09-5,a producer telling you the result.

                                            CAS NO.53075-09-5

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To begin with, let us tell you what is the basic information of N,N,N-Trimethyl-1-ammonium adamantane ?

Like many stuff, it has many synonyms as follows

First, the chemical is very special, some technical indexes as below

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Second, the Synthetic Route we will recommend is the most important for your reference?

First, synthesis line of N,N,N-Trimethyl-1-ammonium adamantane CAS NO.53075-09-5  as follows

The production methods of N, N-trimethyl-1-adamantylammonium hydroxide mainly include the following:

Patent Method 1: This method involves a preparation method of N, N, N-trimethyl-1-adamantylammonium hydroxide, with specific steps including:

Reaction of adamantane and bromine in a mixed solvent produces 1-bromoadamantane amine;

1-bromoadamantylamine reacts with urea in a solvent to produce 1-adamantanamine;

Reaction of 1-adamantane amine with methylation reagent to obtain 1-adamantane dimethylamine;

1-adamantyldimethylamine reacts with tertiary amination reagent in a solvent, and the resulting product is subjected to ion exchange to obtain N, N, N-trimethyl-1-adamantylammonium hydroxide.

This method uses adamantane as the starting material and has the characteristics of low cost and industrialization.

Patent Method 2: This method discloses the synthesis method of N, N, N-trimethyl-1-adamantylammonium halide, which involves adding 1-halogenated adamantyl, trimethylamine, and organic solvent to an autoclave, heating to 50-250 ℃, and conducting a closed reaction for 12-48 hours to obtain the reaction solution. Cool the reaction solution to room temperature, filter to obtain crude N, N, N-trimethyl-1-adamantylammonium halide, wash with organic solvent to obtain pure product. This method has the advantages of fewer reaction steps, mild process, low cost, and high yield, with a yield of over 93%.

Bipolar membrane electrodialysis method: This method involves the preparation of N, N, N-trimethyl-1-adamantylammonium hydroxide by bipolar membrane electrodialysis. By introducing an aqueous solution of N, N, N-trimethyl-1-adamantylammonium hydroxide halide into the raw material chamber, pure water is introduced into the acid chamber and alkali chamber respectively, an aqueous solution of sodium sulfate is introduced into the buffer chamber, and a sulfuric acid solution is introduced into the anode chamber and cathode chamber. The liquid in each compartment circulates through the circulating coil, with a flow rate controlled at 10-50L/h. A direct current electric field is applied to the anode plate and cathode plate, and a constant voltage method is used to control the voltage constant at 10-50V. This method utilizes bipolar membrane electrodialysis technology to prepare N, N, N-trimethyl-1-adamantylammonium hydroxide 4 through an electrolytic process.

Electrolysis method: This method involves a preparation process of adamantyltrimethylammonium hydroxide, which includes two steps: pretreatment and electrolysis. The pretreatment steps include preparing an aqueous solution of adamantyltrimethylammonium chloride, extracting it with dichloromethane, adding it to molecular sieves for stirring and filtering, and obtaining the pretreatment solution. The electrolysis step involves adding the pre-treatment solution to the electrolysis machine to prepare a quaternary ammonium alkaline aqueous solution 5 through the electrolysis process.

These methods provide different approaches to prepare N, N, N-trimethyl-1-adamantylammonium hydroxide, including traditional chemical synthesis methods, electrochemical methods, and bipolar membrane electrodialysis technology, each with its own characteristics and applicable scenarios

Third, what is the usage of  N,N,N-Trimethyl-1-ammonium adamantane  CAS NO.53075-09-5 ?  pleas see below

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The main uses of 1-adamantanyltrimethylammonium hydroxide (CAS number: 53075-09-5) include:

Molecular sieve template agent: mainly used for the synthesis of SSZ-13 molecular sieve, which plays an important role in the catalytic reduction treatment of nitrogen oxides in diesel vehicle exhaust according to the national VI and European VI standards.

Catalyst for organic silicon product polymerization: During the polymerization process of organic silicon products, 1-adamantanyltrimethylammonium hydroxide can be used as a catalyst.

Cleaning agent for the electronics industry: In the electronics industry, it is used as a cleaning agent to remove impurities and contaminants from components.

Phase transfer catalyst: In organic synthesis chemistry, it is used as a phase transfer catalyst to promote the progress of chemical reactions.

Adjusting agent in surfactant products: In the production of surfactants, it is used as an adjusting agent to help adjust the performance of the product.

Polarographic reagents and pH regulators in the field of analytical chemistry: In analytical chemistry, it can be used as a polarographic reagent and pH regulator for precise measurement and analysis of the properties of chemical substances.

In addition, 1-adamantanyltrimethylammonium hydroxide is also used to manufacture new catalysts, especially in the treatment of exhaust gases from automobiles and petroleum. This compound is easily soluble in water and undergoes 100% ionization, with strong alkalinity, so caution should be exercised when using and handling it.

Besides Safety Information of N,N,N-Trimethyl-1-ammonium adamantane  CAS NO.53075-09-5  is also important when handling it

What is the appearance of N,N,N-Trimethyl-1-ammonium adamantane  CAS NO.53075-09-5?   Please see the picture of N,N,N-Trimethyl-1-ammonium adamantane  CAS NO.53075-09-5, below

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Specification of N,N,N-Trimethyl-1-ammonium adamantane  CAS NO.53075-09-5, is below

Apperance: colorless to light yellow liquid

Easy to absorb carbon dioxide, strong alkalinity, and strong corrosiveness.

Assay: 25 min by GC

IR identity: conform

Water:0.5% max by K.F.

Packaging and storage: 25kg/plastic drum, 200kg/plastic drum or ton drum, tank. Store in a dark, cool, dry, and well ventilated place.

Reference of  Article cited for your reference below,

(1)

Catalytic activity of Cu–SSZ-13 prepared with different methods for NH3-SCR reaction

Publication Name: Rare Metals

Publication Date: 2018-11-09

DOI: 10.1007/s12598-018-1143-6

(2)

Cu Loading Dependence of Fast NH3-SCR on Cu/SSZ-13

Publication Name: Emission Control Science and Technology

Publication Date: 2019-03-27

DOI: 10.1007/s40825-019-00117-2

(3)

Time-resolved copper speciation during selective catalytic reduction of NO on Cu-SSZ-13

Publication Name: Nature Catalysis

Publication Date: 2018-03-08

DOI: 10.1038/s41929-018-0032-6